| RULE 412. |
SOIL DECONTAMINATION OPERATIONS |
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(Adopted 1/16/2001) |
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| A. |
Applicability |
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This Rule shall apply to Excavation and/or treatment of ROC-Contaminated Soil. |
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A.1 |
Exemptions |
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The provision of this rule shall not apply to: |
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A.1.a |
Contaminated Soil exposed for the sole purpose of sampling; |
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A.1.b |
Decontamination of less than one cubic yard of Contaminated Soil with 50 ppm or less of ROC; |
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A.1.c |
Soil contaminated solely by an organic liquid having an initial boiling point of 302° F, or higher, as determined
by ASTM D86-78, provided such soil is not heated above ambient temperature and samples of the contaminating liquid
can be obtained; or |
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A.1.d |
Emergency Excavation and/or Decontamination of soil performed by, under jurisdiction of, or pursuant to requirements
of, an authorized health officer, agricultural commissioner, fire protection officer, or other authorized agency
officer. The Air Pollution Control Officer (APCO) shall be notified prior to commencing such Excavation. |
| C. |
Administrative Requirements |
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C.1 |
Test Methods |
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C.1.a |
Initial boiling point of a liquid shall be measured in accordance with ASTM D86. |
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C.1.b |
For purposes of Contaminated Soil and Impervious Barrier (as defined in Rule 101), volatilization of ROC's from
Contaminated Soils shall be measured using a ROC Analyzer which satisfies requirements of U.S. EPA Method 21, 40
CFR Part 60. |
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C.1.c |
Organic Content of soil shall be determined, as appropriate, by U.S. EPA Reference Method 8015, 8260, or the gas
chromatographic method contained in the "Leaking Underground Fuel Tank (LUFT) Manual (October, 1989)"
as approved by the California Department of Health Services. |
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C.2 |
Soil Sampling Procedure (Used in Determining Organic Content) |
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One composite sample shall be collected and analyzed for every 50 cubic yards of excavated Contaminated Soil. (Samples
are not required if soil is not "Contaminated Soil") |
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C.2.a |
A composite sample shall consist of one sample taken from the center of each of the four equal sectors of the area
required to be sampled using procedures described below unless another method is approved by the APCO because the
standard method is infeasible. |
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C.2.b |
Samples shall be taken from at least three inches into the Contaminated Soil of a pile using a driven-tube type
sampler, capped and sealed with inert materials, and extruded in the lab to reduce loss of volatile materials;
or by using a clean brass or stainless steel tube (at least three inches long) driven into the soil with a suitable
instrument. Ends of the tube shall then be covered with aluminum foil, then plastic end caps, and finally wrapped
with a suitable tape. Samples shall be immediately placed on ice, or dry ice, for transport to a laboratory. |
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C.2.c |
Chain-of-custody records shall be kept to document possession of a sample from collection in the field until it
is analyzed. |