Laboratory Standard Operating Procedures for Ambient Air
This page last reviewed July 19, 2012
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The
laboratory standard operating procedures (SOPs) are documents which
describe the steps necessary to conduct a measurement and the critical
parameters to be evaluated during the analysis. SOPs set out
detailed steps that implement the general guidance of the quality
control manual. SOPs are written such that a chemist or
laboratory technician with experience in the particular analytical
technique can follow the procedure and obtain the same result as
another similarly trained chemist. The SOPs are specific to the
Air Resources Board laboratories because they describe the actual
instrumentation and equipment used. Mention of specific equipment
and products do not constitute endorsement or recommendation for use by
the Air Resources Board.
SOPs have been written for each method used by the Air Resources Board to generate data for record. The
listed SOPs are used by the Air Resources Board laboratories to analyze ambient air samples. The following
table provides a summary of each active SOP along with the entire document. Inactive SOPs and their summaries currently not in use are archived for future reference.
Please contact Kathy Gill at (916) 445-9483 or Michael Werst at
(916) 322-6202 for questions or information regarding the Organics
Laboratory and Inorganics Laboratory SOPs, respectively.
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Organics Laboratory
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SOP-Version
Number
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Standard Operating Procedure Title
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Effective
Date
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Summary
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SOP
PDF
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020-3.3
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Cleaning 6-Liter Summa Polished Canisters |
01/01/02
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2K
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178K
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022-4.1
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Determination of Carbonyl Compounds in Ambient Air |
01/01/96
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2K
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133K
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058-2.0
Special Study
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Determination of Aromatic and Halogenated Compounds in Ambient Air by Capillary Column Gas Chromatography/Mass
Spectrometry
Parallel Study of Data from Ambient Air Samples Analyzed by Methods MLD052, MLD057, MLD058, for 1,3-Butadiene,
Aromatic, and Halogenated Compounds |
05/15/02
06/25/02
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5K
3K
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836K
477K
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066-1.0
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Determination of Oxygenates and Nitriles in Ambient Air by Capillary Column Gas Chromatography/Mass Spectrometry |
07/01/03
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4K
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838K
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Inorganics Laboratory
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SOP-Version
Number
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Standard Operating Procedure Title
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Effective
Date
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Summary
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SOP
(PDF)
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005-6.1
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Metals Analysis by Atomic Absorption Spectrophotometry |
5/15/07
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3K
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215K
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007-4.1
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Determination of Sulfate, Nitrate, and Chloride Using Ion Chromatography |
01/19/88
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2K
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N/A
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016-6.0
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Mass Analysis and Subsequent Extraction of SSI-Sampled PM10 from Exposed Quartz Microfiber Filters |
03/21/91
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2K
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244K
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023-1.0
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Determination of Ammonium and Potassium Using Ion Chromatography |
02/01/88
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2K
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N/A
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034-2.0
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Determination of Elemental Concentrations in Ambient Air by Energy-Dispersive X-Ray Fluorescent Spectroscopy |
06/17/91
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2K
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211K
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038-N/A
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Hazardous Waste Disposal Procedure |
Pending
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N/A
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N/A
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039-3.0
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Extraction and Analysis of Hexavalent Chromium by Ion Chromatography |
08/01/93
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3K
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131K
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055-0.0
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Determination of PM2.5 Mass in Ambient Air by Gravimetric Analysis |
07/31/02
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3K
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183K
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061-1.0
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Trace Elemental Analysis of Ambient Air Particulate Samples Using Inductively Coupled Plasma-Mass Spectrometry (ICP-MS) |
01/01/07
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2K
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172K
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062-0.0
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Filter and Canister Preparation for PM2.5 Speciation Samples |
06/20/02
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2K
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128K
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064-0.0
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Analysis of Anions and Cations in PM2.5 Speciation Samples by Ion Chromatography |
06/18/02
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3K
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186K
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065-1.0
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Organic and Elemental Carbon Analysis of Exposed Quartz Microfiber Filters |
08/01/02
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3K
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71K
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Test Methods and Procedures